Technology Process of C36H41N3O7
There total 15 articles about C36H41N3O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C37H43N3O7;
With
lithium hydroxide;
In
tetrahydrofuran;
at 20 ℃;
With
hydrogenchloride;
In
tetrahydrofuran; water;
pH=< 7;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: potassium acetate / acetone
2.1: acetic acid; phosphoric acid / 5 h / Reflux
3.1: trichlorophosphate / 2 h / Reflux
4.1: sodium t-butanolate / dimethyl sulfoxide / 1 h / 0 - 20 °C
4.2: 4 h / 10 °C
4.3: pH 6 - 7
5.1: thionyl chloride / 1 h / Reflux
6.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
7.1: lithium hydroxide / tetrahydrofuran / 20 °C
7.2: pH < 7
With
4-methyl-morpholine; thionyl chloride; phosphoric acid; potassium acetate; benzotriazol-1-ol; acetic acid; HATU; lithium hydroxide; sodium t-butanolate; trichlorophosphate;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetone;
- Guidance literature:
-
Multi-step reaction with 11 steps
1.1: potassium carbonate / butanone / 0.5 h / 20 °C
1.2: 100 °C
2.1: ethanol; water / 5 - 10 °C
3.1: Warmed water bath
4.1: bromine / chloroform
5.1: potassium acetate / acetone
6.1: acetic acid; phosphoric acid / 5 h / Reflux
7.1: trichlorophosphate / 2 h / Reflux
8.1: sodium t-butanolate / dimethyl sulfoxide / 1 h / 0 - 20 °C
8.2: 4 h / 10 °C
8.3: pH 6 - 7
9.1: thionyl chloride / 1 h / Reflux
10.1: benzotriazol-1-ol; 4-methyl-morpholine; HATU / dichloromethane / 20 °C
11.1: lithium hydroxide / tetrahydrofuran / 20 °C
11.2: pH < 7
With
4-methyl-morpholine; thionyl chloride; phosphoric acid; bromine; potassium acetate; potassium carbonate; benzotriazol-1-ol; acetic acid; HATU; lithium hydroxide; sodium t-butanolate; trichlorophosphate;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; water; dimethyl sulfoxide; acetone; butanone;