2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine

Base Information

Chemical Name:2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine
CAS No.:1393815-82-1
Molecular Formula:C₂₆H₂₄N₄O₄S
Molecular Weight:488.567
Hs Code.:

Synonyms:2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine

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Chemical Property of 2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine

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Technology Process of 2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine

There total 7 articles about 2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393816-16-4
5,6,7-trimethoxy-2-(4-(5-(4-methoxy-3-nitrophenyl)-1H-imidazol-1-yl)phenyl)benzo[d]thiazole

: 1393815-82-1
2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine

Guidance literature:: With tin(II) chloride dihdyrate; In ethanol; for 2h; Reflux;

Reference yield:

: 122-04-3
4-nitro-benzoyl chloride

: 1393815-82-1
2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / 3 h / Reflux

2: Lawessons reagent / toluene / 6 h / 110 °C

3: potassium hexacyanoferrate(III); sodium hydroxide / water / 2 h / 90 °C

4: tin(II) chloride dihdyrate / ethanol / 2 h / 80 °C

5: acetic acid / ethanol / 2 h / Reflux

6: potassium carbonate / 1,2-dimethoxyethane; methanol / 12 h / Reflux

7: tin(II) chloride dihdyrate / ethanol / 2 h / Reflux

With Lawessons reagent; pyridine; tin(II) chloride dihdyrate; potassium carbonate; sodium hydroxide; potassium hexacyanoferrate(III); acetic acid; In methanol; 1,2-dimethoxyethane; ethanol; water; toluene;

Reference yield:

: 24313-88-0
3,4,5-Trimethoxyaniline

: 1393815-82-1
2-methoxy-5-(1-(4-(5,6,7-trimethoxybenzo[d]thiazol-2-yl)phenyl)-1H-imidazol-5-yl)benzene amine

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / 3 h / Reflux

2: Lawessons reagent / toluene / 6 h / 110 °C

3: potassium hexacyanoferrate(III); sodium hydroxide / water / 2 h / 90 °C

4: tin(II) chloride dihdyrate / ethanol / 2 h / 80 °C

5: acetic acid / ethanol / 2 h / Reflux

6: potassium carbonate / 1,2-dimethoxyethane; methanol / 12 h / Reflux

7: tin(II) chloride dihdyrate / ethanol / 2 h / Reflux

With Lawessons reagent; pyridine; tin(II) chloride dihdyrate; potassium carbonate; sodium hydroxide; potassium hexacyanoferrate(III); acetic acid; In methanol; 1,2-dimethoxyethane; ethanol; water; toluene;