P(C₆H₅)2CCC₆H₄CN

Base Information

Chemical Name:P(C₆H₅)2CCC₆H₄CN
CAS No.:764663-44-7
Molecular Formula:C₂₁H₁₄NP
Molecular Weight:311.323
Hs Code.:

P(C<sub>6</sub>H<sub>5</sub>)2CCC<sub>6</sub>H<sub>4</sub>CN

Synonyms:P(C₆H₅)2CCC₆H₄CN

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Chemical Property of P(C₆H₅)2CCC₆H₄CN

Chemical Property:

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Technology Process of P(C₆H₅)2CCC₆H₄CN

There total 3 articles about P(C₆H₅)2CCC₆H₄CN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 3032-92-6
4-cyanophenylacetylene

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 764663-44-7
P(C₆H₅)2CCC₆H₄CN

Guidance literature:: With copper(l) iodide; triethylamine; In toluene; Inert atmosphere; Heating;
DOI:10.1055/s-0030-1261223

Reference yield:

: 623-00-7
4-bromobenzenecarbonitrile

: potassium ((Diphenylphosphino)ethynyl)trifluoroborate

: 764663-44-7
P(C₆H₅)2CCC₆H₄CN

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate; In tetrahydrofuran; water; Inert atmosphere; Reflux;
DOI:10.3390/molecules191221324

Reference yield:

: 6104-47-8
ethynyldiphenylphosphine

: 764663-44-7
P(C₆H₅)2CCC₆H₄CN

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 1 h / 0 °C / Inert atmosphere

1.3: 2 h / -10 - 20 °C / Inert atmosphere

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate / tetrahydrofuran; water / Inert atmosphere; Reflux

With n-butyllithium; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; caesium carbonate; In tetrahydrofuran; hexane; water;
DOI:10.3390/molecules191221324