dimethylsulfoxonium methylide*triphenylborane

Base Information

Chemical Name:dimethylsulfoxonium methylide*triphenylborane
CAS No.:502622-28-8
Molecular Formula:C₂₁H₂₃BOS
Molecular Weight:334.29
Hs Code.:

Synonyms:dimethylsulfoxonium methylide*triphenylborane

Suppliers and Price of dimethylsulfoxonium methylide*triphenylborane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethylsulfoxonium methylide*triphenylborane

Chemical Property:

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Technology Process of dimethylsulfoxonium methylide*triphenylborane

There total 1 articles about dimethylsulfoxonium methylide*triphenylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 960-71-4
triphenylborane

: 70775-39-2,5367-24-8
dimethylsulfoxonium methylide

: 502622-28-8
dimethylsulfoxonium methylide*triphenylborane

Guidance literature:: In tetrahydrofuran; (N2); addn. dropwise of soln. of CH2SMe2O (1 equiv.) in THF to stirred suspn. of BPh3 (1 equiv.) in degassed THF at -78°C for 10 min; removal of solvent in vac. over 2 days at -40°C;
DOI:10.1021/om0208568

Reference yield:

: 502622-28-8
dimethylsulfoxonium methylide*triphenylborane

: 1160248-91-8
B(C₆H₅)2(CH₂C₆H₅)

: 67-68-5,8070-53-9
dimethyl sulfoxide

Guidance literature:: In neat (no solvent); heating under N2 atm. at a heating rate of 2.5-10°C/min to 400°C; Kinetics;
DOI:10.1016/j.tca.2004.05.024