Technology Process of C29H37N5O5
There total 4 articles about C29H37N5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate; XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
tert-butyl alcohol;
at 80 ℃;
Inert atmosphere of N2;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethylazodicarboxylate / tetrahydrofuran / 3 h / 20 °C
2: potassium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium(0) / tert-butyl alcohol / 80 °C / Inert atmosphere of N2
With
potassium carbonate; diethylazodicarboxylate; XPhos;
tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran; tert-butyl alcohol;
2: Buchwald-Hartwig Pd catalyzed aryl C-N formation;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / platinum on carbon / thiophene; methanol; di-isopropyl ether / 16 h
2: potassium carbonate; XPhos / tris-(dibenzylideneacetone)dipalladium(0) / tert-butyl alcohol / 80 °C / Inert atmosphere of N2
With
hydrogen; potassium carbonate; XPhos;
tris-(dibenzylideneacetone)dipalladium(0); platinum on carbon;
In
thiophene; methanol; di-isopropyl ether; tert-butyl alcohol;
2: Buchwald-Hartwig Pd catalyzed aryl C-N formation;