1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole

Base Information

Chemical Name:1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole
CAS No.:1451007-63-8
Molecular Formula:C₉H₄N₈O₁₀
Molecular Weight:384.178
Hs Code.:

Synonyms:1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole

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Technology Process of 1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole

There total 3 articles about 1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 4899-39-2
3-chloro-2,4,6-trinitrobenzenamine

: 5213-49-0
2,4-dinitro-1H-imidazole

: 1451007-63-8
1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole

Guidance literature:: 2,4-dinitro-1H-imidazole; With potassium hydrogencarbonate; In isopropyl alcohol; at 20 ℃; for 1h;

3-chloro-2,4,6-trinitrobenzenamine; With tetrabutylammomium bromide; In isopropyl alcohol; at 85 ℃; for 24h;
DOI:10.1039/c3nj00521f

Reference yield:

: 883235-79-8
C₈H₄Cl₂N₄O₇

: 1451007-63-8
1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / ethanol

2.1: potassium hydrogencarbonate / isopropyl alcohol / 1 h / 20 °C

2.2: 24 h / 85 °C

With hydrogenchloride; potassium hydrogencarbonate; In ethanol; isopropyl alcohol;
DOI:10.1039/c3nj00521f

Reference yield:

: 108-42-9
3-chloro-aniline

: 1451007-63-8
1-(3-amino-2,4,6-trinitrophenyl)-2,4-dinitroimidazole

Guidance literature:: Multi-step reaction with 3 steps

2.1: hydrogenchloride / ethanol

3.1: potassium hydrogencarbonate / isopropyl alcohol / 1 h / 20 °C

3.2: 24 h / 85 °C

With hydrogenchloride; potassium hydrogencarbonate; In ethanol; isopropyl alcohol;
DOI:10.1039/c3nj00521f