4-chloro-2-(o-chlorobenzoyl)-N-glycinanilide hydrobromide

Base Information

• Chemical Name: 4-chloro-2-(o-chlorobenzoyl)-N-glycinanilide hydrobromide
• CAS No.: 76337-73-0
• Molecular Formula: BrH*C₁₅H₁₂Cl₂N₂O₂
• Molecular Weight: 404.09
• Mol file: 76337-73-0.mol

Synonyms:4-chloro-2-(o-chlorobenzoyl)-N-glycinanilide hydrobromide

Chemical Property of 4-chloro-2-(o-chlorobenzoyl)-N-glycinanilide hydrobromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-chloro-2-(o-chlorobenzoyl)-N-glycinanilide hydrobromide

There total 1 articles about 4-chloro-2-(o-chlorobenzoyl)-N-glycinanilide hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.8%

4-chloro-2-(o-chlorobenzoyl)-Nα-(benzyloxycarbonyl)glycinanilide (29176-39-4) → 4-chloro-2-(o-chlorobenzoyl)-N-glycinanilide hydrobromide (76337-73-0)

Guidance literature:

With hydrogen bromide; In acetic acid; for 1.5h; Ambient temperature;

DOI:10.1021/jm00133a006

Reference yield: 89.3%

4-chloro-2-(o-chlorobenzoyl)-N-glycinanilide hydrobromide (76337-73-0) + acetyl chloride (75-36-5) → 4-chloro-2-(o-chlorobenzoyl)-Nα-acetylglycinanilide (76337-77-4)

Guidance literature:

In N,N,N,N,N,N-hexamethylphosphoric triamide; for 3h; Ambient temperature;

DOI:10.1021/jm00133a006

upstream raw materials:

4-chloro-2-(o-chlorobenzoyl)-N^α-(benzyloxycarbonyl)glycinanilide

Downstream raw materials:

4-chloro-2-(o-chlorobenzoyl)-N^α-acetylglycinanilide