methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

Base Information

Chemical Name:methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate
CAS No.:1067197-11-8
Molecular Formula:C₁₇H₁₄Cl₂N₄O₂
Molecular Weight:377.23
Hs Code.:

Synonyms:methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

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Chemical Property of methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

Chemical Property:

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Technology Process of methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

There total 6 articles about methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 637-87-6
1-Chloro-4-iodobenzene

: 1067197-08-3
methyl N-[[2-chloro-5-(1H-1,2,3-triazol-5-yl)phenyl]methyl]carbamate

: 1067197-10-7
methyl N-[[2-chloro-5-[2-(4-chlorophenyl)-2H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

: 1067197-11-8
methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

Guidance literature:: With caesium carbonate; copper(II) oxide; iron(III)-acetylacetonate; In N,N-dimethyl-formamide; at 110 ℃; for 14h;

Reference yield:

: 116632-41-8
1-chloro-4-iodo-2-methylbenzene

: 1067197-10-7
methyl N-[[2-chloro-5-[2-(4-chlorophenyl)-2H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

: 1067197-11-8
methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / dichloromethane; water / 2 h / Irradiation

2: potassium carbonate / 1 h / 110 °C

3: triethylamine; triphenylphosphine; copper(l) iodide / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.5 h / 20 °C

4: potassium hydroxide / methanol / 18 h / 20 °C

5: trimethylsilylazide; copper(l) iodide / N,N-dimethyl-formamide; methanol / 8 h / 100 °C / Microwave irradiation

6: caesium carbonate; copper(II) oxide / iron(III)-acetylacetonate / N,N-dimethyl-formamide / 14 h / 110 °C

With N-Bromosuccinimide; copper(l) iodide; 2,2'-azobis(isobutyronitrile); trimethylsilylazide; potassium carbonate; caesium carbonate; triethylamine; triphenylphosphine; copper(II) oxide; potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride; iron(III)-acetylacetonate; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1067197-20-9
methyl [(2-chloro-5-iodophenyl)methyl]carbamate

: 1067197-10-7
methyl N-[[2-chloro-5-[2-(4-chlorophenyl)-2H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

: 1067197-11-8
methyl N-[[2-chloro-5-[1-(4-chlorophenyl)-1H-1,2,3-triazol-4-yl]phenyl]methyl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; triphenylphosphine; copper(l) iodide / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.5 h / 20 °C

2: potassium hydroxide / methanol / 18 h / 20 °C

3: trimethylsilylazide; copper(l) iodide / N,N-dimethyl-formamide; methanol / 8 h / 100 °C / Microwave irradiation

4: caesium carbonate; copper(II) oxide / iron(III)-acetylacetonate / N,N-dimethyl-formamide / 14 h / 110 °C

With copper(l) iodide; trimethylsilylazide; caesium carbonate; triethylamine; triphenylphosphine; copper(II) oxide; potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride; iron(III)-acetylacetonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;