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2-benzyl-2-(pyridin-2-ylthio)nonanedinitrile

Base Information
  • Chemical Name:2-benzyl-2-(pyridin-2-ylthio)nonanedinitrile
  • CAS No.:1510799-57-1
  • Molecular Formula:C21H23N3S
  • Molecular Weight:349.5
  • Hs Code.:
2-benzyl-2-(pyridin-2-ylthio)nonanedinitrile

Synonyms:2-benzyl-2-(pyridin-2-ylthio)nonanedinitrile

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Chemical Property of 2-benzyl-2-(pyridin-2-ylthio)nonanedinitrile
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Technology Process of 2-benzyl-2-(pyridin-2-ylthio)nonanedinitrile

There total 1 articles about 2-benzyl-2-(pyridin-2-ylthio)nonanedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran / 0.25 h / -78 °C
1.2: 2 h / -78 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 0.75 h / -78 °C
2.2: 6 h / -78 - 20 °C
With sodium hydride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ol403020s
Guidance literature:
With n-butyllithium; dibutylmagnesium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 2h;
DOI:10.1021/ol403020s
upstream raw materials:

2-(pyridin-2-ylthio)acetonitrile

Downstream raw materials:

methyl 2-benzyl-2,8-dicyanooctanoate

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