methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane

Base Information

Chemical Name:methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane
CAS No.:124549-79-7
Molecular Formula:C₁₅H₂₉NO₄
Molecular Weight:287.4
Hs Code.:

Synonyms:methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane

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Chemical Property of methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane

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Technology Process of methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane

There total 7 articles about methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 124549-78-6
methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

: 124549-79-7
methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane

Guidance literature:: With hydrogen; Ru-carbon; In tetrahydrofuran; water; for 24h; under 101258 - 127510 Torr; Ambient temperature;

Reference yield:

: 109-04-6
2-bromo-pyridine

: 124549-79-7
methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 1.) BuLi / tetrahydrofuran; hexane / 3 h / -78 °C

2: 92 percent / triethylamine / tetrahydrofuran / 696 h / Heating

3: 93 percent / H₂ / 5percent Ru-C / tetrahydrofuran; H₂O / 24 h / 101258 - 127510 Torr / Ambient temperature

With n-butyllithium; hydrogen; triethylamine; Ru-carbon; In tetrahydrofuran; hexane; water;

Reference yield:

: 56180-50-8
4,4-dimethoxycyclohexan-1-one

: 124549-79-7
methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-piperidyl)cyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 1.) BuLi / tetrahydrofuran; hexane / 3 h / -78 °C

2: 92 percent / triethylamine / tetrahydrofuran / 696 h / Heating

3: 93 percent / H₂ / 5percent Ru-C / tetrahydrofuran; H₂O / 24 h / 101258 - 127510 Torr / Ambient temperature

With n-butyllithium; hydrogen; triethylamine; Ru-carbon; In tetrahydrofuran; hexane; water;