methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

Base Information

Chemical Name:methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane
CAS No.:124549-78-6
Molecular Formula:C₁₅H₂₃NO₄
Molecular Weight:281.352
Hs Code.:

Synonyms:methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

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Chemical Property of methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

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Technology Process of methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

There total 6 articles about methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 124568-67-8
1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

: 107-30-2
chloromethyl methyl ether

: 124549-78-6
methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

Guidance literature:: With triethylamine; In tetrahydrofuran; for 696h; Heating;

Reference yield:

: 109-04-6
2-bromo-pyridine

: 124549-78-6
methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / 1.) BuLi / tetrahydrofuran; hexane / 3 h / -78 °C

2: 92 percent / triethylamine / tetrahydrofuran / 696 h / Heating

With n-butyllithium; triethylamine; In tetrahydrofuran; hexane;

Reference yield:

: 69125-55-9
4-hydroxy-1-methoxy-1-cyclohexene

: 124549-78-6
methoxymethyl ether of 1,1-dimethoxy-4-hydroxy-4-(2'-pyridyl)cyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / p-toluenesulfonic acid / benzene; methanol / 1 h / Ambient temperature

2: 76 percent / CrO₃, pyridine / CH₂Cl₂ / 22 h / Ambient temperature

3: 76 percent / 1.) BuLi / tetrahydrofuran; hexane / 3 h / -78 °C

4: 92 percent / triethylamine / tetrahydrofuran / 696 h / Heating

With pyridine; chromium(VI) oxide; n-butyllithium; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; hexane; dichloromethane; benzene;