2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

Base Information

Chemical Name:2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate
CAS No.:651729-56-5
Molecular Formula:C₃₆H₃₆N₂O₁₃S₄
Molecular Weight:832.951
Hs Code.:

Synonyms:2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

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Chemical Property of 2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

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Technology Process of 2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

There total 1 articles about 2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 651729-55-4
2-(4-tolylsulfonyl)ethyl 4-(2-amino-4-methoxy-phenyl)aminosulfonyl-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 651729-56-5
2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

Guidance literature:: With pyridine; for 20h;

Reference yield: 75.0%

: 651729-56-5
2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

: 86604-75-3
2-(chloromethyl)-4-methoxy-3,5-dimethylpyridine hydrochloride

: 651729-57-6
2-(4-tolylsulfonyl)ethyl 4-[(5-methoxy-([4-methoxy-3,5-dimethyl(2-pyridyl)]methylthio)-benzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate

Guidance literature:: 2-(4-Tolylsulfonyl)ethyl 4-[(2-mercapto-5-methoxybenzimidazolyl)sulfonyl]-2-(2-[4-tolylsulfonyl]ethoxycarbonylmethoxy)phenoxyacetate; 2-(chloromethyl)-4-methoxy-3,5-dimethylpyridine hydrochloride; With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 22 ℃; for 2.5h;

With hydrogenchloride; at 0 ℃;