Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate

Base Information

• Chemical Name: Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate
• CAS No.: 185685-59-0
• Molecular Formula: C₂₅H₂₈O₃
• Molecular Weight: 376.496

Synonyms:Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate

Chemical Property of Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate

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Technology Process of Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate

There total 3 articles about Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) + 3-iodophenyl-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl)methanone (185685-55-6) → Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate (185685-59-0)

Guidance literature:

With tributyl-amine; (2-Tol)23P; palladium diacetate;

DOI:10.1016/S0960-894X(96)00523-9

Reference yield:

3-iodobenzoyl chloride (1711-10-0) → Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate (185685-59-0)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃

2: 74 percent / (2-Tol)23P, Bu₃N / Pd(OAc)2

With aluminium trichloride; tributyl-amine; (2-Tol)23P; palladium diacetate;

DOI:10.1016/S0960-894X(96)00523-9

Reference yield:

1,1,4,4-Tetramethyl-1,2,3,4-tetrahydro-naphthalene (6683-46-1) → Methyl 3-[3-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylate (185685-59-0)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃

2: 74 percent / (2-Tol)23P, Bu₃N / Pd(OAc)2

With aluminium trichloride; tributyl-amine; (2-Tol)23P; palladium diacetate;

DOI:10.1016/S0960-894X(96)00523-9

upstream raw materials:

acrylic acid methyl ester

3-iodophenyl-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthyl)methanone

3-iodobenzoyl chloride

1,1,4,4-Tetramethyl-1,2,3,4-tetrahydro-naphthalene

Downstream raw materials:

3-[3-(5,5,8,8-Tetramethyl-5,6,7,8-tetrahydro-2-naphthylcarbonyl)phenyl]acrylic acid

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