cyclohexyl-(7-cyclohexylimino-4-phenylsulfanyl-cyclohepta-1,3,5-trienyl)amine

Base Information

Chemical Name:cyclohexyl-(7-cyclohexylimino-4-phenylsulfanyl-cyclohepta-1,3,5-trienyl)amine
CAS No.:1229183-79-2
Molecular Formula:C₂₅H₃₂N₂S
Molecular Weight:392.608
Hs Code.:

Synonyms:cyclohexyl-(7-cyclohexylimino-4-phenylsulfanyl-cyclohepta-1,3,5-trienyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cyclohexyl-(7-cyclohexylimino-4-phenylsulfanyl-cyclohepta-1,3,5-trienyl)amine

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Technology Process of cyclohexyl-(7-cyclohexylimino-4-phenylsulfanyl-cyclohepta-1,3,5-trienyl)amine

There total 1 articles about cyclohexyl-(7-cyclohexylimino-4-phenylsulfanyl-cyclohepta-1,3,5-trienyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1229183-89-4
C₁₉H₂₇BrN₂

: 108-98-5
thiophenol

: 1229183-79-2
cyclohexyl-(7-cyclohexylimino-4-phenylsulfanyl-cyclohepta-1,3,5-trienyl)amine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1021/om901012f

Reference yield: 61.0%

: 1229183-79-2
cyclohexyl-(7-cyclohexylimino-4-phenylsulfanyl-cyclohepta-1,3,5-trienyl)amine

: 544-97-8
dimethyl zinc(II)

: 1229183-88-3
5-phenylsulfanyl-N-cyclohexyl-2-(cyclohexylamino)troponiminate zinc methyl

Guidance literature:: In toluene; byproducts: CH4; (Ar); Schlenk technique; soln. of ligand in toluene was slowly added to soln. of Me2Zn in toluene at 0°C; slowly warmed to room temp.; stirred for 3 h; filtered; evapd.; washed (pentane); elem. anal.;
DOI:10.1021/om901012f