1⁴,8⁴-bismethoxy-2²,3³,4²,5³,6²,7³-hexa(tert-butyloxycarbonylmethoxy)-p-octiphenyl

Base Information

• Chemical Name: 1⁴,8⁴-bismethoxy-2²,3³,4²,5³,6²,7³-hexa(tert-butyloxycarbonylmethoxy)-p-octiphenyl
• CAS No.: 406217-66-1
• Molecular Formula: C₈₆H₉₈O₂₀
• Molecular Weight: 1451.71
• Mol file: 406217-66-1.mol

Synonyms:1⁴,8⁴-bismethoxy-2²,3³,4²,5³,6²,7³-hexa(tert-butyloxycarbonylmethoxy)-p-octiphenyl

Chemical Property of 1⁴,8⁴-bismethoxy-2²,3³,4²,5³,6²,7³-hexa(tert-butyloxycarbonylmethoxy)-p-octiphenyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1⁴,8⁴-bismethoxy-2²,3³,4²,5³,6²,7³-hexa(tert-butyloxycarbonylmethoxy)-p-octiphenyl

There total 1 articles about 1⁴,8⁴-bismethoxy-2²,3³,4²,5³,6²,7³-hexa(tert-butyloxycarbonylmethoxy)-p-octiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

4-methoxyphenylboronic acid (5720-07-0) + (4-thiomethoxyphenyl)boronic acid (98546-51-1) + 64,14-diiodo-63,52,43,32,23,13-hexa(tert-butoxycarbonylmethoxy)-p-sexiphenyl (256387-77-6) → 84,14-dimethylsulfanyl-73,62,53,42,33,22-hexa(tert-butoxycarbonylmethoxy)-p-octiphenyl (256387-80-1) + 14,84-bismethoxy-22,33,42,53,62,73-hexa(tert-butyloxycarbonylmethoxy)-p-octiphenyl (406217-66-1) + C86H98O19S (406217-65-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In ethanol; toluene; at 80 ℃; for 48h;

DOI:10.1021/ja017497c

Reference yield:

14,84-bismethoxy-22,33,42,53,62,73-hexa(tert-butyloxycarbonylmethoxy)-p-octiphenyl (406217-66-1) → C62H50O20

Guidance literature:

With trifluoroacetic acid;

DOI:10.1021/ja017497c

upstream raw materials:

4-methoxyphenylboronic acid

(4-thiomethoxyphenyl)boronic acid

6⁴,1⁴-diiodo-6³,5²,4³,3²,2³,1³-hexa(tert-butoxycarbonylmethoxy)-p-sexiphenyl