13h-Benzo[g]indeno[1,2-b]quinoxalin-13-one

Base Information

• Chemical Name: 13h-Benzo[g]indeno[1,2-b]quinoxalin-13-one
• CAS No.: 40114-82-7
• Molecular Formula: C₁₉H₁₀N₂O
• Molecular Weight: 282.301
• NSC Number: 163547
• DSSTox Substance ID: DTXSID20303924
• Wikidata: Q82049432
• ChEMBL ID: CHEMBL3623532
• Mol file: 40114-82-7.mol

Synonyms:13h-benzo[g]indeno[1,2-b]quinoxalin-13-one;40114-82-7;NSC163547;SCHEMBL2681287;CHEMBL3623532;DTXSID20303924;AKOS002084309;NSC-163547;EU-0093731;Z56791571

Chemical Property of 13h-Benzo[g]indeno[1,2-b]quinoxalin-13-one

Chemical Property:

• Vapor Pressure: 1.04E-11mmHg at 25°C
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 282.079312947
• Heavy Atom Count: 22
• Complexity: 464

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C2C=C3C(=CC2=C1)N=C4C5=CC=CC=C5C(=O)C4=N3

Technology Process of 13h-Benzo[g]indeno[1,2-b]quinoxalin-13-one

There total 2 articles about 13h-Benzo[g]indeno[1,2-b]quinoxalin-13-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

indan-1,2,3-trione hydrate (485-47-2) + 2,3-Diaminonaphthalene (771-97-1) → 13H-benzo[g]indeno[1,2-b]quinoxalin-13-one (40114-82-7)

Guidance literature:

In methanol; at 20 ℃;

DOI:10.1016/j.bmcl.2015.06.042

Reference yield:

→ 13H-benzo[g]indeno[1,2-b]quinoxalin-13-one (40114-82-7)

Guidance literature:

Ninhydrin, 2,3-Diaminonaphthalin;

Reference yield:

N-(2-bromophenyl)-N-phenylbenzenamine (78600-31-4) + 13H-benzo[g]indeno[1,2-b]quinoxalin-13-one (40114-82-7) → C37H25N3O

Guidance literature:

N-(2-bromophenyl)-N-phenylbenzenamine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

13H-benzo[g]indeno[1,2-b]quinoxalin-13-one; In tetrahydrofuran; hexane; at -78 - 20 ℃;

DOI:10.1039/c8tc05462b

upstream raw materials:

indan-1,2,3-trione hydrate

2,3-Diaminonaphthalene