N-(2,2-diethoxyethyl)-N-phenyl malonamide 2-(1,3-trimethylene)dithioketal

Base Information

• Chemical Name: N-(2,2-diethoxyethyl)-N-phenyl malonamide 2-(1,3-trimethylene)dithioketal
• CAS No.: 871365-77-4
• Molecular Formula: C₁₈H₂₆N₂O₄S₂
• Molecular Weight: 398.547

Synonyms:N-(2,2-diethoxyethyl)-N-phenyl malonamide 2-(1,3-trimethylene)dithioketal

Chemical Property of N-(2,2-diethoxyethyl)-N-phenyl malonamide 2-(1,3-trimethylene)dithioketal

Chemical Property:

Purity/Quality:

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Technology Process of N-(2,2-diethoxyethyl)-N-phenyl malonamide 2-(1,3-trimethylene)dithioketal

There total 1 articles about N-(2,2-diethoxyethyl)-N-phenyl malonamide 2-(1,3-trimethylene)dithioketal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2,2-diethoxyethyl)-N-phenyl malonamide (871365-73-0) + 1,3-bis(p-toluenesulfonylthio)propane (3866-79-3) → N-(2,2-diethoxyethyl)-N-phenyl malonamide 2-(1,3-trimethylene)dithioketal (871365-77-4)

Guidance literature:

With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 64h;

Reference yield:

N-(2,2-diethoxyethyl)-N-phenyl malonamide 2-(1,3-trimethylene)dithioketal (871365-77-4) → 5-phenyl-1H-1,5-diazepine-2,4-dione 3-(1,3-trimethylene)dithioketal (871365-78-5)

Guidance literature:

With benzenesulfonic acid; In toluene; at 70 ℃; for 0.75h;

upstream raw materials:

N-(2,2-diethoxyethyl)-N-phenyl malonamide

1,3-bis(p-toluenesulfonylthio)propane

Downstream raw materials:

5-phenyl-1H-1,5-diazepine-2,4-dione 3-(1,3-trimethylene)dithioketal

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