(Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate

Base Information

Chemical Name:(Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate
CAS No.:1256493-41-0
Molecular Formula:C₂₇H₂₇NO₅S
Molecular Weight:477.581
Hs Code.:

Synonyms:(Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate

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Chemical Property of (Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate

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Technology Process of (Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate

There total 1 articles about (Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1256493-72-7
tert-butyl 3-(2-(4-methylphenylsulfonamido)phenyl)-3-oxopropanoate

: 100-52-7
benzaldehyde

: 1256493-41-0
(Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate

Guidance literature:: With piperidine; acetic acid; In toluene; at 20 ℃; for 5h; Molecular sieve;
DOI:10.1021/ol102519z

Reference yield: 92.0%

: 1256493-41-0
(Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate

: (R)-tert-butyl 4-hydroxy-2-phenyl-1-tosyl-1,2-dihydroquinoline-3-carboxylate

Guidance literature:: With N-[3,5-bis(trifluoromethyl)phenyl]-N'-[(9R)-6'-methoxycinchonan-9-yl]thiourea; In toluene; at 0 ℃; for 28h; optical yield given as %ee; stereoselective reaction; Molecular sieve;
DOI:10.1021/ol102519z

Reference yield:

: 1256493-41-0
(Z)-tert-butyl 2-(2-(4-methylphenylsulfonamido)benzoyl)-3-phenylacrylate

: (R)-tert-butyl 4-hydroxy-2-phenyl-1-tosyl-1,2-dihydroquinoline-3-carboxylate

: (S)-tert-butyl 4-hydroxy-2-phenyl-1-tosyl-1,2-dihydroquinoline-3-carboxylate

Guidance literature:: With N-[3,5-bis(trifluoromethyl)phenyl]-N'-[(9R)-6'-methoxycinchonan-9-yl]thiourea; In toluene; at 20 ℃; for 5h; optical yield given as %ee; stereoselective reaction; Molecular sieve;
DOI:10.1021/ol102519z