2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)

Base Information

Chemical Name:2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)
CAS No.:1415150-42-3
Molecular Formula:C₁₆H₂₅N₃OS₄
Molecular Weight:403.658
Hs Code.:

Synonyms:2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)

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Chemical Property of 2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)

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Technology Process of 2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)

There total 3 articles about 2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.6%

: 1415150-41-2
2,2'-(4-methoxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)

: 1415150-42-3
2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)

Guidance literature:: 2,2'-(4-methoxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate); With boron tribromide; In dichloromethane; at -78 - 20 ℃; Schlenk technique; Inert atmosphere;

With water; In dichloromethane;
DOI:10.1016/j.polymer.2012.10.006

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1415150-42-3
2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate; potassium iodide / water / 8 h / 100 °C / Schlenk technique; Inert atmosphere

2: trichlorophosphate / 1 h / 100 °C / Cooling with ice

3: potassium iodide / ethanol / 24 h / 60 °C

4: boron tribromide / dichloromethane / -78 - 20 °C / Schlenk technique; Inert atmosphere

With boron tribromide; sodium carbonate; potassium iodide; trichlorophosphate; In ethanol; dichloromethane; water;
DOI:10.1016/j.polymer.2012.10.006

Reference yield:

: 19721-54-1
2-[(2-hydroxyethyl)-(4-methoxyphenyl)amino]ethanol

: 1415150-42-3
2,2'-(4-hydroxyphenylazanediyl)bis(ethane-2,1-diyl)bis(dimethylcarbamodithioate)

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / 1 h / 100 °C / Cooling with ice

2: potassium iodide / ethanol / 24 h / 60 °C

3: boron tribromide / dichloromethane / -78 - 20 °C / Schlenk technique; Inert atmosphere

With boron tribromide; potassium iodide; trichlorophosphate; In ethanol; dichloromethane;
DOI:10.1016/j.polymer.2012.10.006