bidentate phosphino-thiourea ligand

Base Information

• Chemical Name: bidentate phosphino-thiourea ligand
• CAS No.: 261177-72-4
• Molecular Formula: C₂₁H₂₁N₂PS
• Molecular Weight: 364.451

Synonyms:bidentate phosphino-thiourea ligand

Chemical Property of bidentate phosphino-thiourea ligand

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Technology Process of bidentate phosphino-thiourea ligand

There total 1 articles about bidentate phosphino-thiourea ligand which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

phenyl isothiocyanate (103-72-0) + (2-aminoethyl)diphenylphosphane (4848-43-5) → bidentate phosphino-thiourea ligand (261177-72-4)

Guidance literature:

In ethanol; for 1h; Heating;

DOI:10.1016/S0022-328X(99)00615-4

Reference yield: 86.0%

silver trifluoromethanesulfonate (2923-28-6) + bidentate phosphino-thiourea ligand (261177-72-4) → C42H42AgN4P2S2(1+)*CF3O3S(1-)

Guidance literature:

In dichloromethane; at 20 ℃; for 1.5h;

DOI:10.3390/molecules26226891

Reference yield: 84.0%

[Ag(trifluoromethanesulfonate)(PPh3)] (82888-97-9) + bidentate phosphino-thiourea ligand (261177-72-4) → C39H36AgN2P2S(1+)*CF3O3S(1-)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

DOI:10.3390/molecules26226891

upstream raw materials:

phenyl isothiocyanate

(2-aminoethyl)diphenylphosphane

Downstream raw materials:

[(Ph₂PCH₂CH₂NHC(S)NHPh)Rh(1,5-cyclooctadiene)]Cl

[((C₆H₅)2PCH₂CH₂NHC(S)NHC₆H₅)2Pd]⁽²⁺⁾*[CoCl₄]^(2-)=[((C₆H₅)2P(CH₂)2NHC(S)NHC₆H₅)2Pd][CoCl₄]

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