(S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate

Base Information

Chemical Name:(S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate
CAS No.:1351387-34-2
Molecular Formula:C₃₆H₄₄O₆
Molecular Weight:572.742
Hs Code.:

Synonyms:(S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate

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Chemical Property of (S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate

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Technology Process of (S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate

There total 10 articles about (S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 134903-88-1
4'-(6-(acryloyloxy)hexyloxy)biphenyl-4-carboxylic acid

: 73329-06-3
(S)-4-[(1-methylheptyl)oxy]phenol

: 1351387-34-2
(S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate

Guidance literature:: 4'-(6-(acryloyloxy)hexyloxy)biphenyl-4-carboxylic acid; (S)-4-[(1-methylheptyl)oxy]phenol; With dmap; In dichloromethane; for 1.5h; Inert atmosphere; vacuuming;

With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 108497-36-5
(s)-1-benzyloxy-4-[(1-methylheptyl)oxy]benzene

: 1351387-34-2
(S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 11 h / Inert atmosphere; vacuuming

2.1: dmap / dichloromethane / 1.5 h / Inert atmosphere; vacuuming

2.2: 12 h / 20 °C

With dmap; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane;

Reference yield:

: 103-16-2
4-Benzyloxyphenol

: 1351387-34-2
(S)-4-[(1-methylheptyl)oxy]phenol 4'-(6-acryloxyhexyloxy)-[1,1'-biphenyl]-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: triphenylphosphine; diethylazodicarboxylate / dichloromethane / 25 h / 20 °C / vacuuming; Inert atmosphere; ice bath

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 11 h / Inert atmosphere; vacuuming

3.1: dmap / dichloromethane / 1.5 h / Inert atmosphere; vacuuming

3.2: 12 h / 20 °C

With dmap; hydrogen; triphenylphosphine; diethylazodicarboxylate; palladium 10% on activated carbon; In tetrahydrofuran; dichloromethane;