C₃₀H₂₆N₂S

Base Information

• Chemical Name: C₃₀H₂₆N₂S
• CAS No.: 1453494-47-7
• Molecular Formula: C₃₀H₂₆N₂S
• Molecular Weight: 446.616
• Mol file: 1453494-47-7.mol

Synonyms:C₃₀H₂₆N₂S

Chemical Property of C₃₀H₂₆N₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₆N₂S

There total 1 articles about C₃₀H₂₆N₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5,10-ditolyl-16-thia-5,10,15,17-tetrahydrotripyrrin → C30H26N2S (1453494-47-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trichlorophosphate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

1.2: 1.5 h / 20 °C / Inert atmosphere

2.1: zinc; titanium tetrachloride; copper(l) chloride / tetrahydrofuran / 3 h / Inert atmosphere; Reflux

With titanium tetrachloride; copper(l) chloride; zinc; trichlorophosphate; In tetrahydrofuran; dichloromethane; 2.1: |McMurry Reaction;

DOI:10.1002/anie.201209678

Reference yield: 50.0%

C30H26N2S (1453494-47-7) → C30H24N2S (1453494-49-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1002/anie.201209678

Reference yield: 1.6%

ethanol (64-17-5) + C30H26N2S (1453494-47-7) → C32H28N2OS (1453494-48-8)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In chloroform; at 20 ℃;

DOI:10.1002/anie.201209678

Downstream raw materials:

C₃₂H₂₈N₂OS

C₃₀H₂₄N₂S

C₃₁H₂₆N₂OS