bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate

Base Information

Chemical Name:bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate
CAS No.:126290-99-1
Molecular Formula:C₇₈H₁₁₀N₄O₁₂
Molecular Weight:1295.75
Hs Code.:

Synonyms:bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate

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Chemical Property of bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate

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Technology Process of bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate

There total 3 articles about bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 126291-01-8
N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide

: 100-20-9
terephthaloyl chloride

: 126290-99-1
bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate

Guidance literature:: With dmap; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4020(01)89075-X

Reference yield:

: 2567-50-2
N,N-bis-(cyclohexyl)chloroacetamide

: 126290-99-1
bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / anhydrous K₂CO₃, KI / acetone / 40 h / Heating

2: 82 percent / sodium borohydride / methanol / 0.75 h

3: 82 percent / 4-N,N-dimethylaminopyridine, triethylamine / CH₂Cl₂

With dmap; sodium tetrahydroborate; potassium carbonate; triethylamine; potassium iodide; In methanol; dichloromethane; acetone;
DOI:10.1016/S0040-4020(01)89075-X

Reference yield:

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 126290-99-1
bis-(N,N,N',N'-tetrakis-(cyclohexyl)-4-methylene-1,2-phenylenedioxydiacetamido)-1,4-phthalate

Guidance literature:: Multi-step reaction with 4 steps

1: 61 percent / CH₂Cl₂ / 12 h / 25 °C

2: 63 percent / anhydrous K₂CO₃, KI / acetone / 40 h / Heating

3: 82 percent / sodium borohydride / methanol / 0.75 h

4: 82 percent / 4-N,N-dimethylaminopyridine, triethylamine / CH₂Cl₂

With dmap; sodium tetrahydroborate; potassium carbonate; triethylamine; potassium iodide; In methanol; dichloromethane; acetone;
DOI:10.1016/S0040-4020(01)89075-X