N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide

Base Information

Chemical Name:N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide
CAS No.:126291-01-8
Molecular Formula:C₃₅H₅₄N₂O₅
Molecular Weight:582.824
Hs Code.:

Synonyms:N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide

Chemical Property:

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Technology Process of N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide

There total 3 articles about N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 126291-00-7
N,N,N',N'-tetrakis-(cyclohexyl)-4-formyl-1,2-phenylenedioxydiacetamide

: 126291-01-8
N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.75h;
DOI:10.1016/S0040-4020(01)89075-X

Reference yield:

: 2567-50-2
N,N-bis-(cyclohexyl)chloroacetamide

: 126291-01-8
N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / anhydrous K₂CO₃, KI / acetone / 40 h / Heating

2: 82 percent / sodium borohydride / methanol / 0.75 h

With sodium tetrahydroborate; potassium carbonate; potassium iodide; In methanol; acetone;
DOI:10.1016/S0040-4020(01)89075-X

Reference yield:

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 126291-01-8
N,N,N',N'-tetrakis-(cyclohexyl)-4-hydroxymethyl-1,2-phenylenedioxydiacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / CH₂Cl₂ / 12 h / 25 °C

2: 63 percent / anhydrous K₂CO₃, KI / acetone / 40 h / Heating

3: 82 percent / sodium borohydride / methanol / 0.75 h

With sodium tetrahydroborate; potassium carbonate; potassium iodide; In methanol; dichloromethane; acetone;
DOI:10.1016/S0040-4020(01)89075-X