C₃₉H₅₂N₂O₉

Base Information

Chemical Name:C₃₉H₅₂N₂O₉
CAS No.:1350818-22-2
Molecular Formula:C₃₉H₅₂N₂O₉
Molecular Weight:692.85
Hs Code.:

C<sub>39</sub>H<sub>52</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₃₉H₅₂N₂O₉

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Chemical Property of C₃₉H₅₂N₂O₉

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Technology Process of C₃₉H₅₂N₂O₉

There total 13 articles about C₃₉H₅₂N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 932739-33-8
(2S,3S)-2-[(4R,5R)-2,2-dimethyl-5-phenyl-1,3-dioxolan-4-yl]hex-5-en-3-ol

: 1026015-46-2
(S)-2-{3-[(R)-2-Acryloylamino-3-(4-methoxy-phenyl)-propionylamino]-propionyloxy}-4-methyl-pentanoic acid

: 1350818-22-2
C₃₉H₅₂N₂O₉

Guidance literature:: (S)-2-{3-[(R)-2-Acryloylamino-3-(4-methoxy-phenyl)-propionylamino]-propionyloxy}-4-methyl-pentanoic acid; With 2,4,6-trichlorobenzoyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

(2S,3S)-2-[(4R,5R)-2,2-dimethyl-5-phenyl-1,3-dioxolan-4-yl]hex-5-en-3-ol; With dmap; In tetrahydrofuran; at 20 ℃; for 18h;
DOI:10.1016/j.tetlet.2011.09.134

Reference yield:

: 1350818-15-3
C₂₅H₃₄O₇S

: 1350818-22-2
C₃₉H₅₂N₂O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium iodide / acetone / 24 h / Reflux

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

3.1: ozone / dichloromethane / 0.25 h / -78 °C

4.1: diethyl ether / diethyl ether; dichloromethane / 0.75 h / -78 °C

5.1: methanol; toluene-4-sulfonic acid / 6 h / Reflux

6.1: pyridinium p-toluenesulfonate / 3 h / 20 °C

7.1: methanol; potassium carbonate / 2 h / 20 °C

8.1: 5%-palladium/activated carbon; hydrogen / methanol / 3 h

9.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1 h / 20 °C

10.1: potassium tert-butylate / tetrahydrofuran / 0 °C

10.2: 4 h / 0 - 20 °C

11.1: 2,4,6-trichlorobenzoyl chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 - 20 °C

11.2: 18 h / 20 °C

With methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl ether; [bis(acetoxy)iodo]benzene; 2,4,6-trichlorobenzoyl chloride; 5%-palladium/activated carbon; potassium tert-butylate; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; toluene-4-sulfonic acid; ozone; N-ethyl-N,N-diisopropylamine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone; 10.1: Wittig reaction / 10.2: Wittig reaction / 11.1: Yamaguchi esterification / 11.2: Yamaguchi esterification;
DOI:10.1016/j.tetlet.2011.09.134

Reference yield:

: 1350818-16-4
C₁₈H₂₇IO₄

: 1350818-22-2
C₃₉H₅₂N₂O₉

Guidance literature:: Multi-step reaction with 10 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

2.1: ozone / dichloromethane / 0.25 h / -78 °C

3.1: diethyl ether / diethyl ether; dichloromethane / 0.75 h / -78 °C

4.1: methanol; toluene-4-sulfonic acid / 6 h / Reflux

5.1: pyridinium p-toluenesulfonate / 3 h / 20 °C

6.1: methanol; potassium carbonate / 2 h / 20 °C

7.1: 5%-palladium/activated carbon; hydrogen / methanol / 3 h

8.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 1 h / 20 °C

9.1: potassium tert-butylate / tetrahydrofuran / 0 °C

9.2: 4 h / 0 - 20 °C

10.1: 2,4,6-trichlorobenzoyl chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 0 - 20 °C

10.2: 18 h / 20 °C

With methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl ether; [bis(acetoxy)iodo]benzene; 2,4,6-trichlorobenzoyl chloride; 5%-palladium/activated carbon; potassium tert-butylate; hydrogen; pyridinium p-toluenesulfonate; potassium carbonate; toluene-4-sulfonic acid; ozone; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 9.1: Wittig reaction / 9.2: Wittig reaction / 10.1: Yamaguchi esterification / 10.2: Yamaguchi esterification;
DOI:10.1016/j.tetlet.2011.09.134