tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)

Base Information

Chemical Name:tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)
CAS No.:1431972-80-3
Molecular Formula:C₄₅H₄₅NO₆S₃
Molecular Weight:792.053
Hs Code.:

Synonyms:tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)

Suppliers and Price of tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)

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Technology Process of tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)

There total 1 articles about tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 201230-82-2
carbon monoxide

: 1379804-23-5
tris (4-(5-iodothiophen-2-yl)phenyl)amine

: 71-36-3
butan-1-ol

: 1431972-80-3
tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)

Guidance literature:: With palladium diacetate; triethylamine; triphenylphosphine; In N,N-dimethyl-formamide; at 100 ℃; for 30h; under 11251.1 Torr; Inert atmosphere; Autoclave;
DOI:10.1039/c2dt32553e

Reference yield: 70.0%

: 1431972-80-3
tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)

: 1431972-82-5
5,5',5''-(nitrilotris(benzene-4,1-diyl))tris(thiophene-5,2-diyl)trimethanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; Reflux; Inert atmosphere;
DOI:10.1039/c2dt32553e

Reference yield:

: 1431972-80-3
tributyl 5,5',5''-(nitriliotris(benzene-4,1-diyl))tris(thiophene-2-carboxylate)

: 1431972-85-8
tris(4-(5-(chloromethyl)thiophen-2-yl)phenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / Reflux; Inert atmosphere

2: oxalyl dichloride; N,N-dimethyl-formamide / tetrahydrofuran / 0 - 20 °C

With lithium aluminium tetrahydride; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran;
DOI:10.1039/c2dt32553e