Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Base Information

Chemical Name:Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester
CAS No.:115412-97-0
Molecular Formula:C₁₅H₂₀N₂O₃S
Molecular Weight:308.401
Hs Code.:

Synonyms:Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

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Chemical Property of Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

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Technology Process of Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

There total 4 articles about Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 115413-24-6
Dimethyl-carbamic acid 2-oxo-3-phenylsulfanyl-propyl ester

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 115412-97-0
Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Guidance literature:: at 70 ℃; for 1.5h;
DOI:10.1055/s-1987-28113

Reference yield:

: 3111-52-2
potassium thiophenolate

: 115412-97-0
Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. ethanol / 2 h / 0 - 5 °C

2: 71 percent / DMSO, dicyclohexylcarbodiimide (DCC), H₃PO₄ / 15 h / Ambient temperature

3: 89 percent / 1.5 h / 70 °C

With phosphoric acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In ethanol;
DOI:10.1055/s-1987-28113

Reference yield:

: 96426-73-2
Glycidyl N,N-dimethylcarbamate

: 115412-97-0
Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: aq. ethanol / 2 h / 0 - 5 °C

2: 71 percent / DMSO, dicyclohexylcarbodiimide (DCC), H₃PO₄ / 15 h / Ambient temperature

3: 89 percent / 1.5 h / 70 °C

With phosphoric acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In ethanol;
DOI:10.1055/s-1987-28113