Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Base Information

Chemical Name:Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester
CAS No.:119493-26-4
Molecular Formula:C₁₃H₁₅NO₄S
Molecular Weight:281.332
Hs Code.:

Synonyms:Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester

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Chemical Property of Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester

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Technology Process of Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester

There total 1 articles about Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 115412-97-0
Dimethyl-carbamic acid (Z)-4-dimethylamino-2-oxo-3-phenylsulfanyl-but-3-enyl ester

: 119493-26-4
Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; at 100 ℃; for 0.75h;
DOI:10.1055/s-1987-28114

Reference yield: 100.0%

: 119493-26-4
Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester

: 75-36-5
acetyl chloride

: 119493-35-5
Acetic acid (Z)-4-dimethylcarbamoyloxy-3-oxo-2-phenylsulfanyl-but-1-enyl ester

Guidance literature:: With pyridine; In toluene; 1.) 0 deg C, 10 h, 2.) room temp., 3 h;
DOI:10.1055/s-1987-28114

Reference yield:

: 119493-26-4
Dimethyl-carbamic acid (Z)-4-hydroxy-2-oxo-3-phenylsulfanyl-but-3-enyl ester

: 119493-52-6,119493-53-7
Acetic acid (2R,4R)-6-dimethylcarbamoyloxymethyl-2-ethoxy-5-phenylsulfanyl-3,4-dihydro-2H-pyran-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / toluene / 1.) 0 deg C, 10 h, 2.) room temp., 3 h

2: 69 percent / 24 h / 50 °C

With pyridine; In toluene;
DOI:10.1055/s-1987-28114