C₂₃H₂₄N₂O₇

Base Information

Chemical Name:C₂₃H₂₄N₂O₇
CAS No.:138008-41-0
Molecular Formula:C₂₃H₂₄N₂O₇
Molecular Weight:440.453
Hs Code.:

C<sub>23</sub>H<sub>24</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₂₃H₂₄N₂O₇

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Chemical Property of C₂₃H₂₄N₂O₇

Chemical Property:

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Technology Process of C₂₃H₂₄N₂O₇

There total 31 articles about C₂₃H₂₄N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: C₂₄H₂₆N₄O₁₀S

: 138008-41-0
C₂₃H₂₄N₂O₇

Guidance literature:: With N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; water; at 60 ℃; for 0.5h;
DOI:10.1021/ja00027a071

Reference yield:

: 137964-81-9
2-Benzylamino-6-hydroxy-4-methyl-benzoic acid ethyl ester

: 138008-41-0
C₂₃H₂₄N₂O₇

Guidance literature:: Multi-step reaction with 30 steps

1: H₂ / Pd/C / ethanol / 2 h / 23 °C / 62057.8 Torr

2: 1.) aq. NaNO₂, HCl, 2.) NaN₃ / 1.) EtOH, 0 deg C, 20 min, 2.) EtOH, 0 deg C, 40 min

3: i-Pr₂NEt / CH₂Cl₂ / 23 °C

4: NBS, Bz₂O₂ / benzene / 2 h / Heating

5: K₂CO₃ / dimethylformamide / 0.25 h / 70 °C

6: TFA / CH₂Cl₂ / 3 h / 23 °C

7: K₂CO₃ / dimethylformamide / 80 °C

8: 100 percent / DIBAL / CH₂Cl₂ / -78 °C

9: 98 percent / PCC / CH₂Cl₂ / 23 °C

10: toluene / 7 h / 170 °C

11: NaOH / methanol / 23 °C

12: m-CPBA / 4 h / 23 °C

13: ClCOCOCl, DMSO (Swern oxidation)

14: aq. LiOH / tetrahydrofuran / 2 h / 0 °C

15: NaBH₄ / ethanol / -78 - 23 °C

16: 92 percent / imidazole, DMAP / CH₂Cl₂ / 23 °C

17: 64 percent / DIBAL / toluene / -78 °C

18: m-CPBA / CH₂Cl₂ / 23 °C

19: 10 h / 23 °C

20: 83 percent / ClCOCOCl, DMSO (Swern oxidation)

21: H₂NNH₂ / methanol; CH₂Cl₂ / 23 °C

22: n-Bu₄NF / tetrahydrofuran / 23 °C

23: 100 percent / CSA / CH₂Cl₂ / 23 °C

24: aq. NaN₃ / dimethylformamide / 6 h / 125 °C

25: Et₃N / CH₂Cl₂ / 23 °C

26: 1.) TFA, 2.) COCl₂, pyridine / 1.) CH₂Cl₂, 23 deg C, 10 min, 2.) CH₂Cl₂, 23 deg C

27: ceric ammonium nitrate (CAN) / acetonitrile; H₂O / 23 °C

28: PCC, MgSO₄ / CH₂Cl₂ / 23 °C

29: CSA / methanol / 23 °C

30: 71 percent / Ph₃P, i-Pr₂NEt / tetrahydrofuran; H₂O / 0.5 h / 60 °C

With pyridine; 1H-imidazole; hydrogenchloride; dmap; lithium hydroxide; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; sodium azide; oxalyl dichloride; ammonium cerium(IV) nitrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; hydrogen; diisobutylaluminium hydride; magnesium sulfate; potassium carbonate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; pyridinium chlorochromate; trifluoroacetic acid; hydrazine; sodium nitrite; dibenzoyl peroxide; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;
DOI:10.1021/ja00027a071

Reference yield:

: 100-44-7
benzyl chloride

: 138008-41-0
C₂₃H₂₄N₂O₇

Guidance literature:: Multi-step reaction with 24 steps

1: K₂CO₃ / dimethylformamide / 80 °C

2: 100 percent / DIBAL / CH₂Cl₂ / -78 °C

3: 98 percent / PCC / CH₂Cl₂ / 23 °C

4: toluene / 7 h / 170 °C

5: NaOH / methanol / 23 °C

6: m-CPBA / 4 h / 23 °C

7: ClCOCOCl, DMSO (Swern oxidation)

8: aq. LiOH / tetrahydrofuran / 2 h / 0 °C

9: NaBH₄ / ethanol / -78 - 23 °C

10: 92 percent / imidazole, DMAP / CH₂Cl₂ / 23 °C

11: 64 percent / DIBAL / toluene / -78 °C

12: m-CPBA / CH₂Cl₂ / 23 °C

13: 10 h / 23 °C

14: 83 percent / ClCOCOCl, DMSO (Swern oxidation)

15: H₂NNH₂ / methanol; CH₂Cl₂ / 23 °C

16: n-Bu₄NF / tetrahydrofuran / 23 °C

17: 100 percent / CSA / CH₂Cl₂ / 23 °C

18: aq. NaN₃ / dimethylformamide / 6 h / 125 °C

19: Et₃N / CH₂Cl₂ / 23 °C

20: 1.) TFA, 2.) COCl₂, pyridine / 1.) CH₂Cl₂, 23 deg C, 10 min, 2.) CH₂Cl₂, 23 deg C

21: ceric ammonium nitrate (CAN) / acetonitrile; H₂O / 23 °C

22: PCC, MgSO₄ / CH₂Cl₂ / 23 °C

23: CSA / methanol / 23 °C

24: 71 percent / Ph₃P, i-Pr₂NEt / tetrahydrofuran; H₂O / 0.5 h / 60 °C

With pyridine; 1H-imidazole; dmap; lithium hydroxide; sodium hydroxide; sodium tetrahydroborate; sodium azide; oxalyl dichloride; ammonium cerium(IV) nitrate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; magnesium sulfate; potassium carbonate; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; pyridinium chlorochromate; trifluoroacetic acid; hydrazine; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ja00027a071