but-3-en-1-yl 4-(trifluoromethyl)benzoate

Base Information

Chemical Name:but-3-en-1-yl 4-(trifluoromethyl)benzoate
CAS No.:1043963-17-2
Molecular Formula:C₁₂H₁₁F₃O₂
Molecular Weight:244.213
Hs Code.:

Synonyms:but-3-en-1-yl 4-(trifluoromethyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of but-3-en-1-yl 4-(trifluoromethyl)benzoate

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Technology Process of but-3-en-1-yl 4-(trifluoromethyl)benzoate

There total 2 articles about but-3-en-1-yl 4-(trifluoromethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.3%

: 627-27-0
homoalylic alcohol

: 329-15-7
4-trifluoromethyl-phenyl acetyl chloride

: 1043963-17-2
but-3-en-1-yl 4-(trifluoromethyl)benzoate

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 2.5h; Inert atmosphere;
DOI:10.1002/ejoc.201900651

Reference yield: 70.0%

: 1043963-13-8
C₁₂H₁₂BrF₃O₂

: 1043963-17-2
but-3-en-1-yl 4-(trifluoromethyl)benzoate

Guidance literature:: With [(dimethylphenylsilyl)methyl]magnesium chloride; 1,3-bis(mesityl)imidazolium chloride; cobalt(II) chloride; In tetrahydrofuran; 1,4-dioxane; at 25 ℃; for 1.8h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja804277x

Reference yield: 15.0%

: 1043963-17-2
but-3-en-1-yl 4-(trifluoromethyl)benzoate

: 3,5,5,5-tetrafluoropentyl 4-(trifluoromethyl)benzoate

Guidance literature:: With perfluoro-2,4-dimethyl-3-ethylpent-3-yl radical; In 1,2-dichloro-ethane; at 90 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1002/ejoc.201900651