4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate

Base Information

Chemical Name:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate
CAS No.:1262015-14-4
Molecular Formula:C₁₇H₂₁BN₂O₄
Molecular Weight:328.176
Hs Code.:

Synonyms:4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate

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Chemical Property of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate

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Technology Process of 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate

There total 7 articles about 4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 530-62-1
1,1'-carbonyldiimidazole

: 302348-51-2
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

: 1262015-14-4
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate

Guidance literature:: In chloroform; at 25 ℃; for 2h; Solvent; Time; Temperature;

Reference yield: 87.0%

: 288-32-4
1H-imidazole

: 32315-10-9
bis(trichloromethyl) carbonate

: 302348-51-2
(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol

: 1262015-14-4
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate

Guidance literature:: bis(trichloromethyl) carbonate; (4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)methanol; With sodium carbonate; In toluene; at 20 ℃;

1H-imidazole; In toluene; at 20 ℃;
DOI:10.1039/c7sc04318j

Reference yield:

: 59016-93-2
p-hydroxymethylphenylboronic acid

: 1262015-14-4
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzyl 1H-imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate / tetrahydrofuran / 6 h / Reflux; Inert atmosphere

2: dichloromethane / 3 h / 20 °C / Inert atmosphere

With sodium sulfate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201811261