6,7,9,10,12,13,15,16,23,24,26,27,29,30-Tetradecahydrodibenzo[b,N][1,4,7,10,13,16,19,22,25]nonaoxacycloheptacosine

Base Information

Chemical Name:6,7,9,10,12,13,15,16,23,24,26,27,29,30-Tetradecahydrodibenzo[b,N][1,4,7,10,13,16,19,22,25]nonaoxacycloheptacosine
CAS No.:61260-08-0
Molecular Formula:C26H36 O9
Molecular Weight:492.566
Hs Code.:
DSSTox Substance ID:DTXSID20976758
Nikkaji Number:J1.558.217K
ChEMBL ID:CHEMBL1574884
Mol file:61260-08-0.mol

Synonyms:dibenzo-27-crown-9

Suppliers and Price of 6,7,9,10,12,13,15,16,23,24,26,27,29,30-Tetradecahydrodibenzo[b,N][1,4,7,10,13,16,19,22,25]nonaoxacycloheptacosine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,7,9,10,12,13,15,16,23,24,26,27,29,30-Tetradecahydrodibenzo[b,N][1,4,7,10,13,16,19,22,25]nonaoxacycloheptacosine

Chemical Property:

Vapor Pressure:3.34E-15mmHg at 25°C
Boiling Point:632.2°C at 760 mmHg
Flash Point:247.9°C
PSA：83.07000
Density:1.075g/cm³
LogP:2.99860
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:0
Exact Mass:492.23593272
Heavy Atom Count:35
Complexity:453

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCOC2=CC=CC=C2OCCOCCOCCOC3=CC=CC=C3OCCOCCO1

Technology Process of 6,7,9,10,12,13,15,16,23,24,26,27,29,30-Tetradecahydrodibenzo[b,N][1,4,7,10,13,16,19,22,25]nonaoxacycloheptacosine

There total 10 articles about 6,7,9,10,12,13,15,16,23,24,26,27,29,30-Tetradecahydrodibenzo[b,N][1,4,7,10,13,16,19,22,25]nonaoxacycloheptacosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 68822-98-0
2,2'-(2,2'-(2,2'-oxybis(ethane-2,1-diyl)bis(oxy))bis(ethane-2,1-diyl))bis(oxy)diphenol

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 61260-08-0
[2,14]dibenzo-27-crown-9

Guidance literature:: With sodium hydride; In tetrahydrofuran; 4 h, 55 deg C then 16 h, r.t.;

Reference yield:

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 61260-08-0
[2,14]dibenzo-27-crown-9

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / sodium hydride / tetrahydrofuran / 16 h / Heating

2: 98 percent / H₂ / 10percent palladium on carbon / methanol; CH₂Cl₂

3: 54 percent / sodium hydride / tetrahydrofuran / 4 h, 55 deg C then 16 h, r.t.

With hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 112-60-7
Tetraethylene glycol

: 61260-08-0
[2,14]dibenzo-27-crown-9

Guidance literature:: Multi-step reaction with 4 steps

1: 56 percent / pyridine / 2 h

2: 75 percent / sodium hydride / tetrahydrofuran / 16 h / Heating

3: 98 percent / H₂ / 10percent palladium on carbon / methanol; CH₂Cl₂

4: 54 percent / sodium hydride / tetrahydrofuran / 4 h, 55 deg C then 16 h, r.t.

With pyridine; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;