1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione

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Chemical Name:1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione
CAS No.:170804-60-1
Molecular Formula:C₂₁H₂₂N₂O₆
Molecular Weight:398.415
Hs Code.:

Synonyms:1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione

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Chemical Property of 1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione

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Technology Process of 1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione

There total 5 articles about 1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 170804-58-7
3-nitro-4-<(1-oxohexyl)amino>benzoic acid, 2'-acetylphenyl ester

: 170804-60-1
1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione

Guidance literature:: With pyridine; potassium hydroxide; at 60 ℃; for 1h;
DOI:10.1016/0223-5234(96)88270-5

Reference yield:

: 142-61-0
Hexanoyl chloride

: 170804-60-1
1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / dimethylformamide / 3 h / Heating

2: 69 percent / HNO₃(red, fuming) / 0.5 h / -15 °C

3: 96.5 percent / SOCl₂ / tetrahydrofuran / 2 h / Heating

4: 10.6 g / tetrahydrofuran / 1 h / Heating

5: 63 percent / KOH, pyridine / 1 h / 60 °C

With pyridine; potassium hydroxide; thionyl chloride; nitric acid; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(96)88270-5

Reference yield:

: 109506-41-4
4-<(1-oxohexyl)amino>benzoic acid

: 170804-60-1
1-(2-hydroxyphenyl)-3-<3'-nitro-4'-<(1-oxohexyl)amino>phenyl>-1,3-propanedione

Guidance literature:: Multi-step reaction with 4 steps

1: 69 percent / HNO₃(red, fuming) / 0.5 h / -15 °C

2: 96.5 percent / SOCl₂ / tetrahydrofuran / 2 h / Heating

3: 10.6 g / tetrahydrofuran / 1 h / Heating

4: 63 percent / KOH, pyridine / 1 h / 60 °C

With pyridine; potassium hydroxide; thionyl chloride; nitric acid; In tetrahydrofuran;
DOI:10.1016/0223-5234(96)88270-5