(2,3-dihydroxyphenyl)butyl ketone

Base Information

Chemical Name:(2,3-dihydroxyphenyl)butyl ketone
CAS No.:862666-33-9
Molecular Formula:C₁₁H₁₄O₃
Molecular Weight:194.23
Hs Code.:

Synonyms:(2,3-dihydroxyphenyl)butyl ketone

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Chemical Property of (2,3-dihydroxyphenyl)butyl ketone

Chemical Property:

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Technology Process of (2,3-dihydroxyphenyl)butyl ketone

There total 2 articles about (2,3-dihydroxyphenyl)butyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15121-97-8
1-(2,3-dimethoxyphenyl)-1-pentanol

: 862666-33-9
(2,3-dihydroxyphenyl)butyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: Na₂Cr₂O₇; aq. H₂SO₄ / acetone / 3 h / 20 °C

2: 200 mg / BBr₃ / CH₂Cl₂ / 20 °C

With sodium dichromate; sulfuric acid; boron tribromide; In dichloromethane; acetone; 1: Jones oxidation;
DOI:10.1021/ja052326j

Reference yield:

: 86-51-1
2,3-dimethyoxybenzaldehyde

: 862666-33-9
(2,3-dihydroxyphenyl)butyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1.1: Mg / diethyl ether / 0.5 h / Heating

1.2: diethyl ether / 2 h / Heating

2.1: Na₂Cr₂O₇; aq. H₂SO₄ / acetone / 3 h / 20 °C

3.1: 200 mg / BBr₃ / CH₂Cl₂ / 20 °C

With sodium dichromate; sulfuric acid; boron tribromide; magnesium; In diethyl ether; dichloromethane; acetone; 2.1: Jones oxidation;
DOI:10.1021/ja052326j