(E)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone

Base Information

Chemical Name:(E)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone
CAS No.:1353044-37-7
Molecular Formula:C₂₂H₁₈Cl₂F₆N₄O₂
Molecular Weight:555.307
Hs Code.:

Synonyms:(E)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone

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Technology Process of (E)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone

There total 2 articles about (E)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1233037-18-7
1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone

: 1353046-20-4
N-(2,2,2-trifluoroethyl)hydrazinecarboxamide hydrochloride

: 1353043-90-9
(Z)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone

: 1353044-37-7
(E)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone

Guidance literature:: With acetic acid; In ethanol; at 70 ℃; for 6h;

Reference yield:

: 1233037-08-5
4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-benzaldehyde

: 1353043-90-9
(Z)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone

: 1353044-37-7
(E)-1-{4-[5-(3,5-dichloro-phenyl)-5-trifluoromethyl-4,5-dihydro-isoxazol-3-yl]-2-methyl-phenyl}-ethanone-4-trifluoroethylsemicarbazone

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium chloride / toluene; tetrahydrofuran / 1 h / -70 °C

1.2: 20 °C

2.1: Dess-Martin periodane / dichloromethane / 20 °C

2.2: 1 h / 20 °C

3.1: acetic acid / ethanol / 6 h / 70 °C

With Dess-Martin periodane; acetic acid; lithium chloride; In tetrahydrofuran; ethanol; dichloromethane; toluene;