potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate

Base Information

Chemical Name:potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate
CAS No.:84459-83-6
Molecular Formula:C₈H₆N₃O₃S₂*K
Molecular Weight:295.384
Hs Code.:

Synonyms:potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate

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Chemical Property of potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate

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Technology Process of potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate

There total 6 articles about potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 75-15-0,12122-00-8
carbon disulfide

: 636-97-5
N-amino-(4-nitrophenyl)carboxamide

: 84459-83-6
potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate

Guidance literature:: With potassium hydroxide; In ethanol; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.200900218

Reference yield:

: 99-77-4
ethyl 4-nitrobenzoate

: 84459-83-6
potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: 85percent hydrazine / 90 - 95 °C

2: KOH / ethanol / 12 h / 40 °C

With potassium hydroxide; hydrazine hydrate; In ethanol;
DOI:10.1080/00397919808004956

Reference yield:

: 619-50-1
4-nitrobenzoic acid methyl ester

: 84459-83-6
potassium 2-(4-nitrobenzoyl)hydrazinecarbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine hydrate / Reflux

2.1: potassium hydroxide / methanol / 0.25 h

2.2: 3 h / 20 - 25 °C

With hydrazine hydrate; potassium hydroxide; In methanol;