(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

Base Information

Chemical Name:(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate
CAS No.:1610376-69-6
Molecular Formula:C₁₈H₂₉O₃PS₂
Molecular Weight:388.532
Hs Code.:

Synonyms:(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

Suppliers and Price of (Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

There total 3 articles about (Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1610376-65-2
2-phenethyl-2-vinyloxirane

: 107-56-2
O,O-diisopropyl hydrogen phosphorodithioate

: 1610376-69-6
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

: 1610376-72-1
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

Guidance literature:: In toluene; at 20 ℃; for 8h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.04.028

Reference yield:

: 53931-59-2
5-phenyl-1-penten-3-one

: 1610376-69-6
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

: 1610376-72-1
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; diethyl ether / 0.37 h / -100 °C / Inert atmosphere

2: sodium hydride / mineral oil; dimethyl sulfoxide / 20 °C / Inert atmosphere

3: toluene / 8 h / 20 °C / Inert atmosphere

With n-butyllithium; sodium hydride; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.tetlet.2014.04.028

Reference yield:

: 1610376-87-8
C₁₂H₁₅ClO

: 1610376-69-6
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

: 1610376-72-1
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-diisopropyl phosphorodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil; dimethyl sulfoxide / 20 °C / Inert atmosphere

2: toluene / 8 h / 20 °C / Inert atmosphere

With sodium hydride; In dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.tetlet.2014.04.028