1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene

Base Information

Chemical Name:1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene
CAS No.:1332499-13-4
Molecular Formula:C₆₀H₉₈N₁₀O₁₄P₂
Molecular Weight:1245.44
Hs Code.:

1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene

Synonyms:1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene

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Chemical Property of 1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene

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Technology Process of 1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene

There total 9 articles about 1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 935-14-8
1,4-diethynylbenzene

: 1332499-11-2
methyl (6-azidohex-1-yl) [(3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

: 1332499-13-4
1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In toluene; at 80 ℃; for 48h; Inert atmosphere;
DOI:10.1039/c1ob05384a

Reference yield:

: C₆H₁₅N*C₁₉H₃₅N₂O₇P

: 1332499-13-4
1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 1 h / Inert atmosphere

2: copper(l) iodide; N-ethyl-N,N-diisopropylamine / toluene / 48 h / 80 °C / Inert atmosphere

With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In toluene; acetonitrile;
DOI:10.1039/c1ob05384a

Reference yield:

: 1158845-35-2
ammonium [methyl (3R,4R,5S)-4-acetamido-5-(1,1-dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate]

: 1332499-13-4
1,4-bis[1-(hex-1'-yl methyl [(3R,4R,5S)-4-acetamido-5-(1,1dimethylethyloxycarbonylamino)-3-(1-ethylpropoxy)-1-cyclohexene-1-phosphonate])-1H-1,2,3-triazol-4-yl]-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: Amberlite IR-120 / water

2: acetonitrile / 1 h / Inert atmosphere

3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / toluene / 48 h / 80 °C / Inert atmosphere

With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In water; toluene; acetonitrile;
DOI:10.1039/c1ob05384a