C₆₈H₇₇I₂N₃O₇

Base Information

Chemical Name:C₆₈H₇₇I₂N₃O₇
CAS No.:1404213-33-7
Molecular Formula:C₆₈H₇₇I₂N₃O₇
Molecular Weight:1302.18
Hs Code.:

C<sub>68</sub>H<sub>77</sub>I<sub>2</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₆₈H₇₇I₂N₃O₇

Suppliers and Price of C₆₈H₇₇I₂N₃O₇

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₆₈H₇₇I₂N₃O₇

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₈H₇₇I₂N₃O₇

There total 9 articles about C₆₈H₇₇I₂N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1404213-32-6
C₄₆H₅₃NO₃

: 766543-56-0
N-tert-butoxycarbonyl-3,5-diiodoaniline

: 1404213-33-7
C₆₈H₇₇I₂N₃O₇

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/ejoc.201200655

Reference yield:

: 1404213-31-5
C₅₂H₆₉NO₃Si₂

: 1404213-33-7
C₆₈H₇₇I₂N₃O₇

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 2: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655

Reference yield:

: 149505-94-2
tert-butyl (4-hydroxybenzyl)carbamate

: 1404213-33-7
C₆₈H₇₇I₂N₃O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium chlorite; sodium iodide / methanol; water

1.2: 20 °C

2.1: potassium carbonate / acetone / Inert atmosphere; Reflux

3.1: trifluoroacetic acid / dichloromethane / 2 h

3.2: 20 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: sodium iodide; potassium carbonate / acetone / Reflux

6.1: triethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide / tetrahydrofuran / 20 °C / Inert atmosphere

7.1: potassium hydroxide / methanol; tetrahydrofuran / 1 h

7.2: Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

9.1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; copper(l) iodide; tetrabutyl ammonium fluoride; boron tribromide; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium iodide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetone; 6.1: |Sonogashira Cross-Coupling / 7.2: |Sonogashira Cross-Coupling / 9.1: |Sonogashira Cross-Coupling;
DOI:10.1002/ejoc.201200655