4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid

Base Information

Chemical Name:4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid
CAS No.:1427192-07-1
Molecular Formula:C₂₆H₃₃NO₆
Molecular Weight:455.551
Hs Code.:

Synonyms:4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid

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Chemical Property of 4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid

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Technology Process of 4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid

There total 6 articles about 4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1427192-08-2
4-(3-(3,5-cis-dimethylpiperidin-1-yl)-1-(2-hydroxy-4,6-dimethoxyphenyl)-3-oxopropyl)benzoic acid

: 74-88-4
methyl iodide

: 1427192-07-1
4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid

Guidance literature:: 4-(3-(3,5-cis-dimethylpiperidin-1-yl)-1-(2-hydroxy-4,6-dimethoxyphenyl)-3-oxopropyl)benzoic acid; methyl iodide; With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 8h;

With lithium hydroxide; In tetrahydrofuran; methanol; water;

With hydrogenchloride; In water; pH=2;

Reference yield:

: 487-06-9
Limettin

: 1427192-07-1
4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: [2,2]bipyridinyl; palladium diacetate / acetic acid; N,N-dimethyl acetamide / 24 h / 110 °C

2: N,N-dimethyl acetamide / 6 h / 80 °C

3: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C

With [2,2]bipyridinyl; palladium diacetate; potassium carbonate; In N,N-dimethyl acetamide; acetic acid; N,N-dimethyl-formamide;

Reference yield:

: 1427192-78-6
C₁₈H₁₆O₆

: 1427192-07-1
4-(3-(3,5-cis-dimethlpiperidin-1-yl)-3-oxo-1-(2,4,6-trimethoxyphenyl)-propyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl acetamide / 6 h / 80 °C

2: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C

With potassium carbonate; In N,N-dimethyl acetamide; N,N-dimethyl-formamide;