4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine

Base Information

• Chemical Name: 4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine
• CAS No.: 201664-80-4
• Molecular Formula: C₂₀H₂₄ClNO₂S₂
• Molecular Weight: 410.001

Synonyms:4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine

Chemical Property of 4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine

Chemical Property:

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Technology Process of 4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine

There total 3 articles about 4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide (201664-76-8) → 4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine (201664-80-4)

Guidance literature:

With titanium tetrachloride; In dichloromethane; for 0.5h; Ambient temperature;

DOI:10.1016/S0040-4039(97)10472-5

Reference yield:

(E)-cinnamylamine (4335-60-8,4360-51-4,4226-59-9) → 4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine (201664-80-4)

Guidance literature:

Multi-step reaction with 3 steps

1: CH₂Cl₂ / Ambient temperature

2: i-Pr₂NEt, DMAP / CH₂Cl₂ / Ambient temperature

3: 97 percent / TiCl₄ / CH₂Cl₂ / 0.5 h / Ambient temperature

With dmap; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1016/S0040-4039(97)10472-5

Reference yield:

[1-Methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-((E)-3-phenyl-allyl)-amine → 4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine (201664-80-4)

Guidance literature:

Multi-step reaction with 2 steps

1: i-Pr₂NEt, DMAP / CH₂Cl₂ / Ambient temperature

2: 97 percent / TiCl₄ / CH₂Cl₂ / 0.5 h / Ambient temperature

With dmap; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1016/S0040-4039(97)10472-5

upstream raw materials:

4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide

(E)-cinnamylamine

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