4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide

Base Information

• Chemical Name: 4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide
• CAS No.: 201664-76-8
• Molecular Formula: C₂₇H₃₁NO₄S₃
• Molecular Weight: 529.745

Synonyms:4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide

Chemical Property of 4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide

Chemical Property:

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Technology Process of 4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide

There total 4 articles about 4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methylthiomethyl p-tolyl sulfone (59662-65-6) → 4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide (201664-76-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 90 percent / 1.) n-BuLi, H(+); 2.) Ac₂O, DMAP, Et₃N₅

2: CH₂Cl₂ / Ambient temperature

3: i-Pr₂NEt, DMAP / CH₂Cl₂ / Ambient temperature

With dmap; n-butyllithium; acetic anhydride; hydrogen cation; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1016/S0040-4039(97)10472-5

Reference yield:

(E)-cinnamylamine (4335-60-8,4360-51-4,4226-59-9) → 4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide (201664-76-8)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / Ambient temperature

2: i-Pr₂NEt, DMAP / CH₂Cl₂ / Ambient temperature

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1016/S0040-4039(97)10472-5

Reference yield:

1-Methyl-4-((E)-1-methylsulfanyl-prop-1-ene-1-sulfonyl)-benzene (99946-84-6,260547-98-6) → 4-Methyl-N-[1-methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-N-((E)-3-phenyl-allyl)-benzenesulfonamide (201664-76-8)

Guidance literature:

Multi-step reaction with 2 steps

1: CH₂Cl₂ / Ambient temperature

2: i-Pr₂NEt, DMAP / CH₂Cl₂ / Ambient temperature

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1016/S0040-4039(97)10472-5

upstream raw materials:

p-toluenesulfonyl chloride

methylthiomethyl p-tolyl sulfone

(E)-cinnamylamine

1-Methyl-4-((E)-1-methylsulfanyl-prop-1-ene-1-sulfonyl)-benzene

Downstream raw materials:

4-(Chloro-phenyl-methyl)-2-methyl-3-methylsulfanyl-1-(toluene-4-sulfonyl)-pyrrolidine

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