methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

Base Information

Chemical Name:methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside
CAS No.:243642-96-8
Molecular Formula:C₃₆H₄₂O₅Si
Molecular Weight:582.812
Hs Code.:

Synonyms:methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

Suppliers and Price of methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

There total 4 articles about methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 100-39-0
benzyl bromide

: 243642-95-7
methyl 5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

: 243642-96-8
methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1016/S0008-6215(99)00078-6

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 243642-96-8
methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / imidazole / dimethylformamide / 1 h / 60 °C

2: 87 percent / NaH / dimethylformamide / 4 h / 20 °C

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide; 1: Etherification / 2: Etherification;
DOI:10.1016/S0008-6215(99)00078-6

Reference yield:

: 25129-51-5
methyl β-D-arabinofuranoside

: 243642-96-8
methyl 2,3-di-O-benzyl-5-O-tert-butyldiphenylsilyl-β-D-arabinofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / imidazole / dimethylformamide / 1 h / 60 °C

2: 87 percent / NaH / dimethylformamide / 4 h / 20 °C

With 1H-imidazole; sodium hydride; In N,N-dimethyl-formamide; 1: Etherification / 2: Etherification;
DOI:10.1016/S0008-6215(99)00078-6