C₉H₆ClNO₃

Base Information

• Chemical Name: C₉H₆ClNO₃
• CAS No.: 1350726-60-1
• Molecular Formula: C₉H₆ClNO₃
• Molecular Weight: 211.605
• Mol file: 1350726-60-1.mol

Synonyms:C₉H₆ClNO₃

Chemical Property of C₉H₆ClNO₃

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₉H₆ClNO₃

There total 1 articles about C₉H₆ClNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C9H8ClNO3 (1269219-36-4) → C9H6ClNO3 (1350726-60-1)

Guidance literature:

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1039/c1ob06274c

Reference yield: 94.0%

C9H6ClNO3 (1350726-60-1) + 1-butyl-3-methylimidazolium thiocyanate (344790-87-0) → 2-(4-chlorophenyl)-3-nitro-4-thiocyanatothietane

Guidance literature:

With sodium O,O-diethyl phosphorodithioate; In tetrahydrofuran; mineral oil; at 20 ℃; for 4.5h; diastereoselective reaction; Inert atmosphere;

DOI:10.1016/j.tet.2012.01.062

Reference yield: 91.0%

[bmim]SPh (1027355-70-9) + C9H6ClNO3 (1350726-60-1) → 2-(4-chlorophenyl)-3-nitro-4-(phenylthio)thietane

Guidance literature:

With sodium O,O-diethyl phosphorodithioate; In tetrahydrofuran; mineral oil; at 20 ℃; for 4.5h; diastereoselective reaction; Inert atmosphere;

DOI:10.1016/j.tet.2012.01.062

upstream raw materials:

C₉H₈ClNO₃