19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine

Base Information

• Chemical Name: 19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine
• CAS No.: 62995-08-8
• Molecular Formula: C₂₇H₂₈N₂O₆
• Molecular Weight: 476.529
• Mol file: 62995-08-8.mol

Synonyms:19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine

Chemical Property of 19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine

There total 8 articles about 19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-benzyloxycarbonyl-9,10-dihydro-9,10-dimethyl-9,10-epoxyiminoanthracene (63044-78-0) + thebaine (115-37-7) → 19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine (62995-08-8)

Guidance literature:

In benzene; for 5h; Heating;

Reference yield: 95.0%

Benzyl N-hydroxycarbamate (3426-71-9) + thebaine (115-37-7) → 19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine (62995-08-8)

Guidance literature:

With benzyltrimethylammonium periodate; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; for 2h;

DOI:10.1021/jo052016j

Reference yield: 66.0%

benzyloxycarbonyl azide (3422-03-5) + thebaine (115-37-7) → Benzyl (dimethyl(oxo)-λ6-sulfaneylidene)carbamate (62995-07-7) + benzaldehyde (100-52-7) + 19-benzyloxycarbonyl-6,14-dihydro-6β,14β-epoxyiminothebaine (62995-08-8)

Guidance literature:

In dimethyl sulfoxide; at 130 ℃; for 5h;

upstream raw materials:

Benzyl N-hydroxycarbamate

thebaine

benzyloxycarbonyl azide

N-benzyloxycarbonyl-9,10-dihydro-9,10-dimethyl-9,10-epoxyiminoanthracene