C₂₁H₃₈O₄Si

Base Information

Chemical Name:C₂₁H₃₈O₄Si
CAS No.:1254369-10-2
Molecular Formula:C₂₁H₃₈O₄Si
Molecular Weight:382.616
Hs Code.:

C<sub>21</sub>H<sub>38</sub>O<sub>4</sub>Si

Synonyms:C₂₁H₃₈O₄Si

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Chemical Property of C₂₁H₃₈O₄Si

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Technology Process of C₂₁H₃₈O₄Si

There total 9 articles about C₂₁H₃₈O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1254369-09-9
C₂₁H₃₆O₂Si

: 1254369-10-2
C₂₁H₃₈O₄Si

Guidance literature:: With potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 36h; optical yield given as %ee;
DOI:10.1021/ml1002184

Reference yield: 91.0%

: C₂₁H₃₆O₂Si

: 1254369-10-2
C₂₁H₃₈O₄Si

Guidance literature:: With AD-Mix-α; optical yield given as %ee; stereoselective reaction;
DOI:10.1021/jo201319b

Reference yield:

: 117643-47-7
C₁₃H₁₈O₂

: 1254369-10-2
C₂₁H₃₈O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 36 h / Reflux

2: lithium aluminium tetrahydride / diethyl ether / 0.17 h / 0 °C / Inert atmosphere

3: 1H-imidazole / N,N-dimethyl-formamide / 16 h / Inert atmosphere

4: potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 36 h / 0 °C

With 1H-imidazole; potassium osmate(VI) dihydrate; lithium aluminium tetrahydride; methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III); In diethyl ether; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 1: Johnson-Claisen orthoester rearrangement / 4: Sharpless dihydroxylation;
DOI:10.1021/ml1002184