(2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanoic acid

Base Information

• Chemical Name: (2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanoic acid
• CAS No.: 1006369-91-0
• Molecular Formula: C₂₇H₃₁NO₆
• Molecular Weight: 465.546

Synonyms:(2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanoic acid

Chemical Property of (2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanoic acid

Chemical Property:

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Technology Process of (2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanoic acid

There total 1 articles about (2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyl (2S,3S)-4-(benzyloxy)-3-[bis(4-methoxybenzyl)amino]-2-hydroxybutanoate (497847-05-9) → (2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanoic acid (1006369-91-0)

Guidance literature:

With sodium hydroxide; In methanol; at 0 - 20 ℃;

DOI:10.1016/j.carres.2007.10.001

Reference yield: 75.0%

(2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanoic acid (1006369-91-0) + 6-amino-6-deoxy-1,2:3,4-di-O-isopropylidene-α-L-galactopyranose (70932-45-5) → N1-(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)-(2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanamide (1006369-94-3)

Guidance literature:

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.carres.2007.10.001

upstream raw materials:

methyl (2S,3S)-4-(benzyloxy)-3-[bis(4-methoxybenzyl)amino]-2-hydroxybutanoate

Downstream raw materials:

N1-(1,2:3,4-di-O-isopropylidene-6-deoxy-α-L-galactopyranos-6-yl)-(2S,3S)-4-(benzyloxy)-3-[di(4-methoxybenzyl)amino]-2-hydroxybutanamide

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