Technology Process of C23H22F3NO3Se2
There total 6 articles about C23H22F3NO3Se2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetone;
at 20 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride; pyridine / ethanol / 2 h / Inert atmosphere; Reflux
2.1: tetrahydrofuran / 12.83 h / 20 - 80 °C / Reflux
2.2: 0.33 h / 20 °C
3.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere
4.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 1 h / 20 °C
5.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C
5.2: 0.17 h / -78 °C
6.1: potassium carbonate / acetone / 4 h / 20 °C
With
pyridine; hydrogenchloride; N-chloro-succinimide; isopropylmagnesium chloride; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetrahydrofuran / 12.83 h / 20 - 80 °C / Reflux
1.2: 0.33 h / 20 °C
2.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere
3.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 1 h / 20 °C
4.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C
4.2: 0.17 h / -78 °C
5.1: potassium carbonate / acetone / 4 h / 20 °C
With
N-chloro-succinimide; isopropylmagnesium chloride; diisobutylaluminium hydride; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; hexane; dichloromethane; acetone;
