5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole

Base Information

Chemical Name:5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole
CAS No.:1337553-43-1
Molecular Formula:C₂₇H₂₁N₃OSe
Molecular Weight:482.443
Hs Code.:

Synonyms:5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole

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Chemical Property of 5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole

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Technology Process of 5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole

There total 6 articles about 5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1337553-30-6
5-iodo-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole

: 5720-07-0
4-methoxyphenylboronic acid

: 1337553-43-1
5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole

Guidance literature:: 5-iodo-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole; 4-methoxyphenylboronic acid; With palladium diacetate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h; Inert atmosphere;

With potassium phosphate; In water; N,N-dimethyl-formamide; for 12h; Reflux; Inert atmosphere;
DOI:10.1055/s-0030-1260083

Reference yield:

: 1236252-96-2
(2-azidophenyl) (phenyl) selenide

: 1337553-43-1
5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(II) acetate monohydrate; sodium L-ascorbate / tetrahydrofuran; water / 12 h / 20 °C / Air

2.1: palladium diacetate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 12 h / Reflux; Inert atmosphere

With palladium diacetate; copper(II) acetate monohydrate; sodium L-ascorbate; In tetrahydrofuran; water; N,N-dimethyl-formamide; 1.1: Huisgen 1,3-dipolar cycloaddition / 2.1: Suzuki cross-coupling reaction / 2.2: Suzuki cross-coupling reaction;
DOI:10.1055/s-0030-1260083

Reference yield:

: 1666-13-3
diphenyl diselenide

: 1337553-43-1
5-(4-methoxyphenyl)-4-phenyl-1-[2-(phenylselanyl)phenyl]-1H-1,2,3-triazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium tetrahydroborate / ethanol; dimethyl sulfoxide

2.1: ammonium chloride; zinc / tetrahydrofuran

3.1: isopentyl nitrite / tetrahydrofuran / 0 °C

3.2: 0 - 20 °C / under air

4.1: copper(II) acetate monohydrate; sodium L-ascorbate / tetrahydrofuran; water / 12 h / 20 °C / Air

5.1: palladium diacetate / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

5.2: 12 h / Reflux; Inert atmosphere

With sodium tetrahydroborate; palladium diacetate; copper(II) acetate monohydrate; ammonium chloride; sodium L-ascorbate; zinc; isopentyl nitrite; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 4.1: Huisgen 1,3-dipolar cycloaddition / 5.1: Suzuki cross-coupling reaction / 5.2: Suzuki cross-coupling reaction;
DOI:10.1055/s-0030-1260083