PtCl₂(1-(diphenylphosphino)-3-(phenylphosphino)propane)

Base Information

• Chemical Name: PtCl₂(1-(diphenylphosphino)-3-(phenylphosphino)propane)
• CAS No.: 88496-13-3
• Molecular Formula: C₂₁H₂₂Cl₂P₂Pt
• Molecular Weight: 602.339

Synonyms:PtCl₂(1-(diphenylphosphino)-3-(phenylphosphino)propane)

Chemical Property of PtCl₂(1-(diphenylphosphino)-3-(phenylphosphino)propane)

Chemical Property:

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Technology Process of PtCl₂(1-(diphenylphosphino)-3-(phenylphosphino)propane)

There total 2 articles about PtCl₂(1-(diphenylphosphino)-3-(phenylphosphino)propane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

dichloro(1,5-cyclooctadiene)platinum(ll) (12080-32-9) + Diphenyl<3-(phenylphosphino)propyl>phosphin (57322-05-1) → (+/-)-dichloro(1-(diphenylphosphino)-3-(phenylphosphino)propane)platinum(II) (88496-13-3)

Guidance literature:

In toluene; benzene; to slurry of Pt complex in C6H6 added soln. of ligand in toluene under N2; concd. in stream of N2, added Et2O, filtered, washed with Et2O, recrystd. (MeNO2); elem. anal.;

DOI:10.1021/ja00333a036

Reference yield: 83.0%

dichloro(1,5-cyclooctadiene)platinum(ll) (12080-32-9) + Diphenyl<3-(phenylphosphino)propyl>phosphin (57322-05-1) → PtCl2(1-(diphenylphosphino)-3-(phenylphosphino)propane) (88496-13-3)

Guidance literature:

In toluene; benzene; under N2 atm. slurry PtCl2(COD) in benzene treated with toluene soln. ppH; mixt. filtered, filtrate reduced in stream N2, Et2O added, product filtered; washed with Et2O and recrystd. from CH3NO2; elem. anal.;

Reference yield: 96.0%

(+/-)-dichloro(1-(diphenylphosphino)-3-(phenylphosphino)propane)platinum(II) (88496-13-3) → (PtCl(C6H5)2P(CH2)3P(C6H5))2

Guidance literature:

With triethylamine; In tetrahydrofuran; to stirred suspn. of Pt complex in THF added NEt3, stirred for 12 h under N2; filtered, washed with abs. EtOH, dried;

DOI:10.1021/ja00333a036

upstream raw materials:

dichloro(1,5-cyclooctadiene)platinum(ll)

Diphenyl<3-(phenylphosphino)propyl>phosphin

Downstream raw materials:

(PtCl((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)3P(C₆H₅)2))⁽¹⁺⁾*AsF₆^(1-)=(PtCl((C₆H₅)2P(CH₂)2P(C₆H₅)(CH₂)3P(C₆H₅)2))AsF₆

(PtCl((C₆H₁₁)2P(CH₂)3P(C₆H₅)(CH₂)3P(C₆H₅)2))⁽¹⁺⁾*AsF₆^(1-)=(PtCl((C₆H₁₁)2P(CH₂)3P(C₆H₅)(CH₂)3P(C₆H₅)2))AsF₆

(PtCl(PhP(CH₂CH₂CH₂PPh₂)2))Cl

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